By C. David Gutsche (auth.), J. Vicens, V. Böhmer (eds.)
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Additional info for Calixarenes: A Versatile Class of Macrocyclic Compounds
R" m m m n m - n-2 Scheme 1. Stepwise synthesis of calix[n]arenes according to Hayes and Hunter  and Kammerer and Happel [2-8]. Table I. Calixarenes synthesized by the stepwise synthesis according to Scheme 1. p. (0C) 320 309 300 343 344 329 332-3 407-9 304 255 265 370 352 360 355 lit. [2,4] [3,4] [3,4]       [3,8]       * Obtained according to Scheme 2. ** Obtained according to Scheme 4. 12, 14, ... steps for calixarenes with 4, 5, 6, ... phenolic units, if the halogenation is regarded as the first step).
3, 65 (1982). Y. Nakamoto and S. Ishida: Makromol. , Rapid Commun. 3, 705 (1982). SYNTHESIS AND PROPERTIES OF CALIXARENES 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30. 31. 32. 33. 34. 35. 36. 37. 38. 39. 40. 41. 42. 43. 44. 45. 46. 47. 48. 49. 49b. 50. 51. 52. 53. 54. 55. 56. 57. 58. 59. 35 C. D. Gutsche and I. Alam: unpublished work. C. D. Gutsche and D. Stewart: unpublished work. S. R. Izatt, R. T. Hawkins, J. J. Christensen, and R. M. Izatt: J. Arn. Chern. Soc. 107,63 (1985). J. W. Cornforth, E.
C. D. Gutsche, K. A. See, and F. Fronczek: unpublished work. C. D. Gutsche and K. C. Nam: J. Arn. Chern. Soc. 110, 6153 (1988). C. D. Gutsche and I. Alam: Tetrahedron 44, 4689 (1988). B. T. Hayes and R. F. Hunter: Chern. Ind. 193 (1956); idem, J. Appl. Chern. 8, 743 (1958). A. Arduini, A. Casnati, A. Pochini, and R. Ungaro: Fifth International Symposium on Inclusion Phenomena and Molecular Recognition, Orange Beach, Alabama, p. H13 (1988); M. Almi, A. Arduini, A. Casnati, A. Pochini, and R. Ungaro: Tetrahedron 45, 2177 (1989).